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Determination of hydrogen sulfide carbonyl sulfide methanethiol and dimethyl sulfide in coal-based syngas -- Gas chromatograph
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GB/T 33443-2016
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PDF similar to GB/T 33443-2016
Basic data | Standard ID | GB/T 33443-2016 (GB/T33443-2016) | | Description (Translated English) | Determination of hydrogen sulfide carbonyl sulfide methanethiol and dimethyl sulfide in coal-based syngas -- Gas chromatograph | | Sector / Industry | National Standard (Recommended) | | Classification of Chinese Standard | G86 | | Classification of International Standard | 71.040.40 | | Word Count Estimation | 10,126 | | Date of Issue | 2016-12-30 | | Date of Implementation | 2017-07-01 | | Regulation (derived from) | National Standard Notice No.27 of 2016 | | Issuing agency(ies) | General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China |
GB/T 33443-2016: Determination of hydrogen sulfide carbonyl sulfide methanethiol and dimethyl sulfide in coal-based syngas -- Gas chromatograph ---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of hydrogen sulfide carbonyl sulfide methanethiol and dimethyl sulfide in coal-based syngas - Gas chromatograph
ICS 71.040.40
G86
National Standards of People's Republic of China
Coal-based synthesis of hydrogen sulfide, carbonyl sulfur,
Determination of mercaptan and methyl sulfide - Gas chromatographic method
Determination ofhydrogensulfidecarbonylsulfidemethanethioland
2016-12-30 release
2017-07-01 implementation
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China
China National Standardization Management Committee released
Foreword
This standard is drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some of the contents of this document may involve patents. The issuer of this document does not assume responsibility for the identification of these patents.
This standard is proposed and centralized by the National Coal Chemical Industry Standardization Technical Committee (SAC/TC469).
The drafting unit. Shenhua Ningxia Coal Industry Group Co., Ltd., National Coal and Coal Chemical Products Quality Supervision and Inspection Center, Shanxi
Jincheng Anthracite Mining Group Co., Ltd. Tianxi Coal & Oil Company.
The main drafters of this standard. Zhi Jianning, Liu Yuqi, Hou Li, Zhao Jianbin, Liu Lei, Luo Jintao, Li Jinkai, Zhou Guang
Coal-based synthesis of hydrogen sulfide, carbonyl sulfur,
Determination of mercaptan and methyl sulfide - Gas chromatographic method
1 Scope
This standard has determined the use of gas detector with flame photometric detector (FPD) determination of coal-based synthesis of hydrogen sulfide, carbonyl sulfur, methyl sulfide
Alcohols, methyl sulfide methods, reagents and materials, apparatus, sampling, assay steps, results calculations, precision, and test reports.
This standard applies to coal-based syngas hydrogen sulfide concentration of not less than 0.08mg/m3, carbonyl sulfide concentration of not less than 0.12mg/m3, methyl sulfide
Alcohol concentration of not less than 0.08mg/m3, methyl sulfide concentration of not less than 0.07mg/m3 determination.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
GB/T 3634.2 Hydrogen - Part 2. Hydrogen, high - purity hydrogen and ultrapure hydrogen
General rules for sampling safety of industrial chemical products GB/T 3723
GB/T 5274 Preparation of gas mixtures for gas analysis calibration
General rules for sampling of gas chemical products GB/T
Representation and Judgment of Numerical Correction Rule and Limit Value of GB/T 8170
GB/T 8979 pure nitrogen, high purity nitrogen and ultra pure nitrogen
GB/T 13277 (all parts) Compressed air
3 terms and definitions
The following terms and definitions apply to this document.
3.1
Coal - based syngas
The main components are hydrogen, carbon monoxide,
Carbon and so on.
3.2
Dilutegasism
The gas used to dilute the high concentration of the sample is usually the same gas as the carrier gas.
4 method summary
The coal-based syngas is passed through a sulfur passivation treatment sample system, separated by column chromatography, flame photometric detector, to retain the time qualitative
Quantitative analysis of external standard method.
5 reagents and materials
5.1 Carrier gas, gas, dilution gas. high purity hydrogen, purity not less than GB/T 3436.2 requirements.
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