Search result: GB/T 1346-2024 (GB/T 1346-2011 Older version)
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Test methods for water requirement of standard consistency, setting time and soundness of the Portland cement
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GB/T 1346-2011 | English | 85 |
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Test methods for water requirement of normal consistency, setting time and soundness of the Portland cement
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GB/T 1346-2001 | English | 359 |
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Test methods for water requirement of normal consistency, setting time and soundness of the Portland cements
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GB/T 1346-1989 | English | 279 |
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Standard test method--Water requirement for normal consistency, setting time and soundness of the portland cement
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Standard ID | GB/T 1346-2024 (GB/T1346-2024) | Description (Translated English) | Test methods for water requirement of standard consistency, setting time and soundness of the portland cement | Sector / Industry | National Standard (Recommended) | Classification of Chinese Standard | Q11 | Classification of International Standard | 91.100.10 | Word Count Estimation | 18,176 | Date of Issue | 2024-12-31 | Date of Implementation | 2025-07-01 | Older Standard (superseded by this standard) | GB/T 1346-2011 | Issuing agency(ies) | State Administration for Market Regulation, National Standardization Administration |
GB/T 1346-2024.Test methods for water consumption, setting time and stability of cement of standard consistency
ICS 91.100.10
CCSQ11
National Standard of the People's Republic of China
Replaces GB/T 1346-2011
Water consumption, setting time and cement standard consistency
Stability test method
Released on 2024-12-31
2025-07-01 Implementation
State Administration for Market Regulation
The National Standardization Administration issued
Table of Contents
Preface III
1 Range 1
2 Normative references 1
3 Terms and Definitions 1
4 Principle 1
5 Instruments and Equipment 2
6 Test water 6
7 Test conditions 7
8 Standard Consistency Water Determination Method---Test Rod Method (Benchmark Method) 7
9 Method for determination of water consumption for standard consistency --- test cone method (substitute method) 7
10 Method for determination of setting time 8
11 Stability determination method---Ray's method (standard method) 9
12 Stability determination method---test cake method (substitute method) 9
13 Inspection Report 10
Preface
This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for standardization work Part 1.Structure and drafting rules for standardization documents"
Drafting.
This document replaces GB/T 1346-2011 "Test methods for water consumption, setting time and stability of cement standard consistency" and is consistent with
Compared with GB/T 1346-2011, in addition to structural adjustments and editorial changes, the main technical changes are as follows.
a) Added “Terms and Definitions” (see Chapter 3);
b) Added relevant technical requirements for “Automatic coagulation time measuring instrument” (see 5.3);
c) The completion time and operation steps of the pure slurry mold filling have been changed (see 8.3, 7.3 of the.2011 edition);
d) The operating time requirements for the standard consistency water content determination method (substitute method) have been changed (see 9.3.2, 10.3.2 of the.2011 edition);
e) The description of the test specimen preparation operation has been changed (see 10.2, 8.2 of the.2011 edition);
f) The operating requirements for the Vicat apparatus method for determining the setting time have been changed (see 10.3, 10.4 and 10.5, 8.3, 8.4 and
8.5);
g) The requirements for stability determination by the Reye's method have been changed (see Chapter 11, Chapter 9 of the.2011 edition);
h) Added the requirement of "If abnormality is observed in the Reye's clamp specimen during moisture curing, terminate the test" and the requirement of "Reye's method stability test before boiling"
Compliance determination for sexual performance (see 11.2.3);
i) Added the requirement of "If obvious cracks are observed on the test cake during moisture curing, terminate the test" (see 12.2);
j) Added the determination of the conformity of the test sample before boiling for stability test using the cake method (see 12.4.1, 11.3.3 of the.2011 edition).
Please note that some of the contents of this document may involve patents. The issuing organization of this document does not assume the responsibility for identifying patents.
This document was proposed by China Building Materials Federation.
This document is under the jurisdiction of the National Cement Standardization Technical Committee (SAC/TC184).
This document was drafted by. China Building Materials Science Research Institute Co., Ltd., China Construction Xinjiang Construction Engineering (Group) Co., Ltd., China Yangtze River
China Three Gorges Corporation, Suzhou Jiaotong University, Zhejiang Yicheng Testing Co., Ltd., China Construction Eighth Engineering Bureau Fourth Construction Co., Ltd.,
Beijing Xingkun Construction Co., Ltd., Henan China Construction Western Construction Co., Ltd., Sujiaoke Group Testing and Certification Co., Ltd., Shanghai Municipal Highway
Engineering Testing Co., Ltd., Shanghai Academy of Building Research Co., Ltd., Sinosteel Zhengzhou Metal Products Research Institute Co., Ltd.,
Shanghai Construction Machinery Testing Center Co., Ltd., Yunnan Building Materials Product Quality Inspection Institute, China Railway First Survey and Design Institute Group Co., Ltd.
Co., Ltd., Hubei Provincial Transportation Planning and Design Institute Co., Ltd., CCCC Second Navigation Engineering Bureau Co., Ltd., Foshan Sanshui District Construction Engineering
Quality Inspection Station, China National Materials Construction Co., Ltd., Zhejiang Institute of Geophysical Technology Application Co., Ltd., Wuhan Zhonghe Engineering Technology Co., Ltd.
Xiamen Jiehang Engineering Testing Technology Co., Ltd., Jiangsu Shanhe Cement Co., Ltd., Shenyang Chengke Engineering Testing Consulting Co., Ltd., Ningxia Construction
Zhixin Testing Co., Ltd., China Railway Construction Bridge Engineering Bureau Group Co., Ltd., Guangzhou Jiyechangqing New Materials Co., Ltd., China Communications Construction Group
Beijing Testing Technology Co., Ltd., Hubei Provincial Construction Engineering Quality Supervision, Inspection and Testing Center Co., Ltd., Shaanxi Zhengchuang Engineering Testing Co., Ltd.
Sinohydro Corporation, China Hydropower No. 11 Engineering Bureau Co., Ltd., Anhui Provincial Construction Engineering Quality Supervision and Inspection Station Co., Ltd., Beijing Shunxin Tianyu Construction
Engineering Co., Ltd., CCCC Central South Engineering Bureau Co., Ltd., Zhejiang Provincial Construction Engineering Quality Inspection Station Co., Ltd., PowerChina Shandong
Electric Power Construction Co., Ltd., Beijing Biboliye Technology Testing Co., Ltd., Shaanxi Hantong Construction Engineering Quality Testing Co., Ltd., Jiangshan He
Jiashan Cement Co., Ltd., Tiezheng Testing Technology Co., Ltd., China Power Construction Group Northwest Survey and Design Institute Co., Ltd., Zhongda Intelligent Technology
Technology Co., Ltd., China Railway 18th Bureau Group Co., Ltd., Wuxi Jianglin Construction Engineering Quality Inspection Co., Ltd., Shanxi Huajian Construction Engineering
Testing Co., Ltd., Wuhan Product Quality Supervision and Inspection Building Materials Station, China Railway Major Bridge Engineering Group Co., Ltd., China Railway 17th Bureau Group Second Engineering Co., Ltd.
Co., Ltd., Shanxi Transportation Science and Technology Research and Development Co., Ltd., Jiangsu Chaoli Building Materials Technology Co., Ltd., China Communications First Highway Engineering Bureau Haiwei Engineering Construction Co., Ltd.
China Railway Jingcheng Engineering Testing Co., Ltd., China Construction Second Engineering Bureau Co., Ltd., China Railway 20th Bureau Group Co., Ltd., Shanxi Fourth Construction Group
Group Co., Ltd., Gansu Zhitong Technology Engineering Testing Consulting Co., Ltd., Xinjiang Midong Tianshan Cement Co., Ltd., Nantong Construction Engineering
Quality Inspection Station Co., Ltd., China Railway Fourth Engineering Bureau Group Co., Ltd., China Railway Shanghai Engineering Bureau Group Co., Ltd., Shanghai Tongji Testing Technology Co., Ltd.
Company, Heilongjiang Province Building Materials Industry Planning and Design Institute, Shenzhen Yuedake Engineering Testing Technology Co., Ltd., China Railway Construction Group
Second Construction Co., Ltd., Tianjin PetroChina Boxing Engineering Technology Co., Ltd., Shandong Highway Design Consulting Co., Ltd., Jiangxi Transportation Investment Group
Group Co., Ltd., Wenzhou Huaxing Building Materials Testing Co., Ltd., Guangzhou Cheng'an Road and Bridge Testing Co., Ltd., China Railway 14th Bureau Group Fourth Engineering
Co., Ltd., Guangdong Guangye Inspection and Testing Group Co., Ltd., Wenzhou Zhengcheng Engineering Quality Inspection Co., Ltd., Deqing Nanfang Cement Co., Ltd.
Company, Zhejiang Zhenghao Engineering Research Co., Ltd., Yitai (Zhuji) Intelligent Equipment Co., Ltd., Poly Changda Engineering Co., Ltd., Suzhou Xiang
Cheng Testing Co., Ltd., Ningxia Zhongce Measurement Testing and Inspection Institute (Co., Ltd.), Jinyu Energy Saving Technology (Tianjin) Co., Ltd., Yangxin Washi
Green Building Materials Co., Ltd., Jidong Cement Tongchuan Co., Ltd., CCCC Second Highway Engineering Bureau Co., Ltd., Jiangsu Construction Engineering Building Materials Quality Inspection
Center Co., Ltd., China Railway 24th Bureau Group Co., Ltd., Mianyang Vocational and Technical College, Shanxi Yellow River New Chemical Co., Ltd., Wuxi Dongyi
MANUFACTURING TECHNOLOGY LIMITED.
The main drafters of this document are. Du Yong, Pan Meichen, Liu Chen, Li Wenwei, Liu Ruihai, Gao Lin, Xu Tongxin, Zhu Wenshang, Wang Junhua, Liu Xiangshun,
Jin Hao, Huang Li, Jiang Lizhen, Wang Xiulan, Wang Shuyuan, Yuan Song, Zheng Xuwei, Xia Zhonglei, Wang Wenwen, Luan Xinguo, Li Yanan, He Guowei, Lü Haisheng,
Sun Sheng, Wang Changan, Zhang Guozhi, Liu Dawei, Shen Dongming, Ren Tao, Mao Weiqi, Zhu Xueren, Kong Haixia, Yang Lei, Xie Jiangsheng, Wu Jianghua, Lv Jinhui,
Wang Zhiling, Li Xuan, Li Xiangsong, Meng Shuling, Chang Ying, Huang Jianshan, Yuan Liang, Ji Jiaxing, Si Jianing, Zhang Xiaodong, Chen Mi, Hua Jun, Wu Wenbo, Liu Hongtao,
Zhao Zhenping, Jiang Feng, Liu Deping, Zhang Chaoyang, Xu Hongxiang, Yu Xiaoqing, Wang Yage, Song Tao, Zhu Yixiang, Bu Fanmin, Li Xiaofeng, Hu Xinying, Wang Lili,
Wang Mingjian, Zhang Shaoshan, Zhang Xinsheng, Xu Zhenxing, Zhang Jiayuan, Ren Sihao, Cao Tingwei, He Zujun, Xu Haihua, Zhang Chunyang, Fan Yongkang, Sun Kai, Jiang Yong,
Chen Risheng, Hu Jian, Yue Yongxiu, Liao Lin, Li Yanqing, Wang Cheng, Zhang Jixin, Yang Haibing, Li Yongchun, Cao Jianming, Zhang Sicai, Zhu Kai, Wang Jun, Wei Ying,
Li Fan, Xiong Linqiang, Chen Ziyang, Dai Gang, Guo Zigang, Zhang Qingshan, Liu Jun, Li Zhitang, Xu Wei, Tao Ying, Wu Xiaosheng, Lei Zhen, Wang Yang, Chen Kun, Yu Yong,
Shen Litao, Liang Long, Zou Hua, Xue Cheng, Shi Weiji, Luo Jixiang, Feng Hao, He Lixin, Xiao Xiaoxuan, Zhang Xinhua, Wang Xi, Guo Zhongyi, Feng Long, Lu Chao,
Yang Huamei and Zhang Sijia.
This document was first issued in 1989, revised for the first time in.2001, revised for the second time in.2011, and this is the third revision.
Water consumption, setting time and cement standard consistency
Stability test method
1 Scope
This document specifies the test method for cement standard consistency water consumption, setting time and volume stability mainly caused by free calcium oxide, etc.
Principles, instruments and equipment, test water, test conditions and measurement methods.
This document is applicable to the test of water consumption, setting time and stability of standard consistency of general Portland cement.
2 Normative references
The contents of the following documents constitute the essential clauses of this document through normative references in this document.
For referenced documents without a date, only the version corresponding to that date applies to this document; for referenced documents without a date, the latest version (including all amendments) applies to
This document.
GB/T 6682 Specifications and test methods for water used in analytical laboratories
GSB14-1510 Cement Standard Sample for Strength Test
JC/T 727 Cement paste standard consistency and setting time tester
JC/T 729 Cement paste mixer
JC/T 954 Levitra clamp for cement stability test
JC/T 955 Boiling chamber for cement stability test
JC/T 962 Leclerc clamp expansion tester
3 Terms and definitions
3.1
When the cement paste reaches the standard consistency, the percentage of water used for mixing the paste in the mass of cement.
3.2
Setting time
The time required for the test needle to sink into the slurry to a certain depth when the cement slurry reaches standard consistency.
Note. Includes initial setting time and final setting time.
3.3
Soundness
The ability of cement paste to maintain a stable volume after hardening.
Note. Characterized by Reye's method or test cake method.
4 Principle
4.1 Standard consistency of cement
Cement paste of standard consistency has a certain resistance to the sinking of standard test rod (or test cone).
......
ICS 91.100.10
Q 11
NATIONAL STANDARD
OF THE PEOPLE’S REPUBLIC OF CHINA
Replacing GB/T 1346-2001
Test methods for Water Requirement of
Normal Consistency, Setting Time and
Soundness of the Portland Cement
(ISO 9597. 2008, Cement - Test Methods - Determination of Setting
Time and Soundness, NEQ)
ISSUED ON. JUNE 20, 2011
IMPLEMENTED ON. MARCH 1, 2012
Jointly Issued by. General Administration of Quality Supervision,
Inspection and Quarantine (AQSIQ);
Standardization Administration (SAC) of the People's
Republic of China.
GB
3. No action is required - Full-copy of this standard will be automatically &
immediately delivered to your EMAIL address in 0~60 minutes.
Foreword
This standard was drafted according to the rules specified in GB/T 1.1-2009.
This standard replaces GB/T 1346-2001 "Test Methods for Water Requirement of
Normal Consistency, Setting Time and Soundness of the Portland Cements"
Compared with GB/T 1346-2001, the main changes of this standard are as follows.
- "Each mould shall be equipped with a flat glass plate larger than the mould and at least
2.5 mm thick" is changed into "each mould shall be equipped with a flat glass base-plate or
metal base-plate with the side length or diameter of about 100mm and thickness of 4mm~
5mm" (see 4.2 of this standard and 4.2 of 2001 edition )
- As for graduated cylinder or burette, "the minimal graduation is 0.1mL and the
precision is 1%" is changed into "the precision is ±0.5mL" (see 4.7 of this standard and 4.7 of
2001 edition);
- "After mixing, the cement paste must be loaded into the mould on the glass plate at
once. The cement paste should be pug, vibrated lightly several times and screeded smoothly."
is changed into "Immediately after mixing, the cement paste of right amount shall be loaded
into the mould on the glass base-plate at a time; remove the voids in the paste by gently
tapping the slightly overfilled mould five times with a straight-edged knife of about 25 mm in
width, and then slightly incline the straight-edged knife to the mould and gently saw the
excessive paste outward at the point about 1/3 of the upper surface of the mould, and then
plaster the top again from the edge for having a smooth surface. During sawing the excessive
paste and screeding, paste shall not be compacted" (see 7.3 of this standard and 7.3 of 2001
edition.)
- "When the initial/final setting time arrived, the repeat of the tests should be done at
once. When the results of two time tests were same as each other, the result can be determined
as initial/final setting time." is changed into "When the initial setting time arrived, the repeat
of the tests should be done at once. When the results of two time tests were same as each
other, the result can be determined as initial setting time. When the final time arrives, the final
setting time can be confirmed by repeating the test in two other positions. The final setting
time is determined to be reached when the results of two times are the same" (See 8.5 of this
standard and 8.5 of 2001 edition);
- "Two glass plates (75 g ~ 85 g/glass plate) are prepared for one Le Chatelier. " is
changed into "Two glass plates of 80mm in side length or diameter and 4mm~ 5mm in
thickness shall be prepared for one Le Chatelier" (See 9.1 of this standard and 9.1 of 2001
edition);
- "pug the cement paste with knife (about 10 mm in width) several times using the other
hand." is changed into "pug the paste surface with knife (about 25 mm in width) three times
using the other hand" (see 9.2 of this standard and 9.2 of 2001 edition);
- "After mixing, the cement paste must be loaded into the mould at once. The cement
paste should be pug, vibrated lightly several times and screeded smoothly." is changed into
"After mixing, the cement paste shall be loaded into cone mould at once. The paste surface
should be pug and vibrated lightly 5 times with a straight-edge knife of about 25 mm in
width." (see 10.3.2 of this standard and 10.3.2 of 2001 edition);
- "When the adjustment approach on amount of water is used, the normal consistency of
cement paste must be accordant with the consistency obtained when the dropping depth of the
test cone is 28 mm ± 2 mm." is changed into "When the adjustment approach on amount of
water is used, the normal consistency of cement paste must be accordant with the consistency
obtained when the dropping depth of the test cone is 30mm± 1mm" (see 10.3.3 of this
standard and 10.3.3 of 2001 edition).
This standard is corresponding to ISO 9597. 2008 "Cement-Test methods-Determination
of setting time and soundness", but not equivalent to it.
This standard was proposed by China Building Materials Federation.
This standard is under the jurisdiction of the National Technical Committee on Cements
of Standardization Administration of China (SAC/TC 184).
Chief Drafting Organizations. China Building Materials Academy, Xiamen Iso Standard
Sand Co., Ltd., Zhejiang Zhongfu Construction Group Co., ltd.
Participating drafting organizations. Xinjiang Tianshan Cement Co., Ltd., Sichuan
Esheng Cement Group Co., Ltd, Yunnan Hongta Dianxi Cement Co., Ltd., Yunnan Kunsteel
Cement Building Materials Group Co., Ltd., LuQuan QuZhai Cement Co., Ltd., Zhongcai
Hanjiang Cement Co., Ltd., Cement Plant of Jizhong Energy Resources Co., Ltd., Shaanxi
Shengwei Building materials Group Co., Ltd., Guangling Jinghua Chemical Group Co., Ltd.,
Henan Tongli cement Co., Ltd., Yunnan Xingjian Cement Co., Ltd., Ningxia Saima industry
Co., Ltd., Hefei Cement Research & Design Institute, Cement Quality Supervisior & test
laboratory of ShanDong Province, Guangdong Building Material Research Institute, Xuzhou
Institute for Products Quality Supervision and Inspection.
Chief drafting staffs. Jiang Lizhen, Liu Chen, Yan Bilan, Cui Xiangyang, Xiao
Zhongming, Zhu Wengao, Li Shengtai, Liu Ge, Yu Ligang, Xu Juehui, Wang Yongqing, Xia
Zhongyong, Wang Jianxin.
The previous editions of the standards replaced by this standard are as.
- GB/T 1346-1989;
- GB/T 1346-2001.
Contents
1 Scope .. 1
2 Normative References .. 1
3 Principle... 1
4 Instruments and Equipment.. 2
5 Materials... 4
6 Testing Conditions ... 4
7 Determination Methods for Water Requirement of Normal Consistency (Standard Method)
... 5
8 Determination Method of Setting Time ... 5
9 Determination of Soundness (Standard Method) ... 7
10 Determination Methods for Water Requirement of Normal Consistency (Replacement
Method) ... 7
11 Determination of Soundness (Replacement Method)... 8
12 Test Report ... 9
1Test methods for Water Requirement of Normal Consistency,
Setting Time and Soundness of the Portland Cement
1 Scope
This standard specifies the principle, instruments and equipment, materials, test
conditions and determination methods of test methods for water requirement of normal
consistency, setting time and volume soundness (caused by free calcium oxide) of the
portland cements.
This method is applicable to portland cement and ordinary portland cement, portland slag
cement, portland fly-ash cement, portland pozzolana cement, composite portland cement and
other cements specified to adopt this method.
2 Normative References
The following referenced documents are indispensable for the application of this
document. For dated references, only the edition cited applies. For undated references, the
latest edition of the referenced document (including any amendments) applies.
JC/T 727 Apparatus for determining normal consistency and setting time of cement paste
JC/T 729 Mixer for cement paste
JC/T 955 Boiling box for determining soundness of cement
3 Principle
3.1 Normal consistency of portland cements
Cement paste of normal consistency has a specified resistance to the dropping of a
standard test bar (or test cone). The water required for such a paste shall be determined by
testing the penetrations of pastes with different water contents.
3.2 Setting time
The setting time is the time required for a needle to drop into the cement paste of normal
consistency for a certain depth.
3.3 Soundness
3.3.1 Le Chatelier is used to indicate the volume expansion of cement paste of normal
consistency by determining the relative displacement of two needles boiled in Le Chatelier.
3.3.2 Pat method is used to indicate the volume soundness by observing the overall change
of paste pat of normal consistency.
5humidity shall not be less than 90%.
7 Determination Methods for Water Requirement of Normal
Consistency (Standard Method)
7.1 Preparation Work before Test
7.1.1 The sliding bar of Vicat apparatus can slip freely. Mould and glass base-plate shall be
cleaned with wet cloth, and mould shall be placed on the base-plate.
7.1.2 The pointer shall indicate the Zero when the test bar is adjusted to touch the glass
plate;
7.1.3 The mixer shall operate normally.
7.2 Mixing the cement paste
Use mixer to mix cement paste. clean the agitator kettle and agitator blade with wet cloth,
pour water into the agitator kettle, add 500g cement into water within 5s~ 10s, prevent water
and cement from spilling; place the agitator kettle on the base of agitator, raise it to the
mixing position, start the mixer and mix at low speed for 120s; scrap cement paste on blade
and kettle wall into the kettle, and then mix at high-speed for 120s before stopping.
7.3 Determination procedure of water requirement of normal consistency
Immediately after blending, the cement paste of right amount shall be loaded into the
mould on the glass base-plate at a time; remove the voids in the paste by gently tapping the
slightly overfilled mould five times with a straight-edged knife of about 25 mm in width, and
then slightly incline the straight-edged knife to the mould and gently saw the excessive paste
outward at the point about 1/3 of the upper surface of the mould, and then plaster the top
again from the edge for having a smooth surface. During sawing the excessive paste and
screeding, paste shall not be compacted. Then the mould and base-plate shall be rapidly
moved on to the Vicat apparatus, and the center of the mould shall be located under the test
bar and the test bar shall be lowered to the surface of cement paste. The screw shall be
tightened for 1s ~ 2s, then released suddenly so the test bar may drop into the cement paste
freely and vertically. After the test bar stopped dropping or was released for 30 s, the distance
between the test bar and base-plate shall be recorded. After test bar is raised, the test bar
should be cleaned at once. The whole operation shall be finished within 1.5min after mixing.
The normal consistency of cement paste shall be accordant with the consistency obtained
when the test bar is dropped into the cement paste with the distance 6 mm ± 1 mm from the
base-plate. The quantity of water for mixing is the water requirement of normal consistency
of cement (P). The unit is the percent according to the mass of cement.
8 Determination Method of Setting Time
8.1 Preparation work before test
When the pointer of instrument for measuring setting time is adjusted to touch the glass
6
plate, the pointer shall indicate Zero.
8.2 Preparation of sample
After the cement paste of normal consistency is made according to the water requirement
of normal consistency and 7.2 and loaded in the mould and scraped according to 7.3, it shall
be moved into humidity-maintenance box. The time when the cements are totally added into
the water shall be recorded as the initial setting time.
8.3 Determination of initial setting time ...
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