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GB 1886.210-2016 English PDF

GB 1886.210-2016_English: PDF (GB1886.210-2016)
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GB 1886.210-2016English190 Add to Cart 0--9 seconds. Auto-delivery National Food Safety Standard -- Food Additives -- Propionic acid Valid GB 1886.210-2016
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BASIC DATA
Standard ID GB 1886.210-2016 (GB1886.210-2016)
Description (Translated English) National Food Safety Standard -- Food Additives -- Propionic acid
Sector / Industry National Standard
Classification of Chinese Standard X09
Word Count Estimation 12,163
Date of Issue 2016-08-31
Date of Implementation 2017-01-01
Regulation (derived from) Announcement of the State Administration of Public Health and Family Planning 2016 No.11


GB 1886.210-2016 GB NATIONAL STANDARD OF THE PEOPLE’S REPUBLIC OF CHINA National food safety standard - Food additives - Propionic acid ISSUED ON: AUGUST 31, 2016 IMPLEMENTED ON: JANUARY 01, 2017 Issued by: National Health and Family Planning Commission of PRC Table of Contents 1 Scope ... 3 2 Chemical name, molecular formula, structural formula, relative molecular mass ... 3 3 Technical requirements ... 3 Appendix A Testing method ... 5 National food safety standard - Food additives - Propionic acid 1 Scope This standard applies to propionic acid, which is refined by industrial synthesis. 2 Chemical name, molecular formula, structural formula, relative molecular mass 2.1 Chemical name Propionic acid 2.2 Molecular formula C3H6O2 2.3 Structural formula 2.4 Relative molecular mass 74.08 (according to 2013 international relative atomic mass) 3 Technical requirements 3.1 Sensory requirements Sensory requirements shall comply with Table 1. Appendix A Testing method A.1 Warning Some reagents used in the test methods of this standard are toxic or corrosive. Appropriate safety and protective measures shall be taken during operation. A.2 General provisions Unless other requirements are specified, the reagents and water used in this standard refer to analytically pure reagents and grade-3 water specified in GB/T 6682. The standard solutions, standard solutions for impurity determination, preparations and products used in the test shall be prepared, in accordance with the provisions of GB/T 601, GB/T 602, GB/T 603, unless other requirements are indicated. The solutions used in the test refer to aqueous solutions, unless the solvent used to prepare them is specified. A.3 Identification test Take 1 mL of specimen. Add 3 drops of sulfuric acid and 1 mL of ethanol. Heat it. It shall have an aromatic smell. A.4 Determination of propionic acid A.4.1 Reagents and materials A.4.1.1 Phenolphthalein indicator solution: 1% ethanol solution. A.4.1.2 Standard titration solution of sodium hydroxide: c (NaOH) = 0.5 mol/L. A.4.2 Analytical procedures Weigh 1.5 g of specimen, accurate to 0.0002 g. Put it into a 250 mL conical flask. Add 100 mL of newly boiled and cooled water. Add 2 drops of phenolphthalein indicator. Use sodium hydroxide standard titration solution to titrate, until red color does not fade for 30 s, which is taken as the end point. A.4.3 Result calculation The mass fraction w1 of propionic acid content is calculated according to formula (A.1): Where: V0 - The volume of iodine standard titration solution, which is consumed during the blank test, in milliliters (mL); V1 - The volume of iodine standard titration solution, which is consumed when measuring the aldehyde content in the specimen, in milliliters (mL); M - The molar mass of propionaldehyde, in grams per mole (g/mol) [M (C3H6O) = 58.08]; m - The mass of the specimen, in grams (g); 1000 - Conversion factor; 2 - Molar conversion factor. The test results are based on the arithmetic mean of parallel measurement results (retaining 3 decimal places). The absolute difference between two independent determination results, which are obtained under repeatability conditions, is not greater than 10% of the arithmetic mean. A.6 Determination of easy oxidants (calculated as formic acid) A.6.1 Reagents and materials A.6.1.1 Sodium hydroxide. A.6.1.2 Bromine. A.6.1.3 Sodium acetate solution: 200 g/L. A.6.1.4 Potassium iodide solution: 250 g/L. A.6.1.5 Hydrochloric acid. A.6.1.6 Sodium thiosulfate standard titration solution: c (Na2S2O3) = 0.1 mol/L. A.6.2 Analytical procedures Dissolve 15 g of sodium hydroxide in 50 mL water. Cool it. Add 6 mL of bromine. Stir thoroughly to dissolve completely. Use water to dilute to 2000 mL. Take 25.0 mL of this solution and place it in a 250 mL stoppered conical flask, which contains 100 mL of water. Add 10 mL of sodium acetate solution and 10 g of specimen (accurate to 0.001 g). Leave it for 15 minutes. Add 5 mL of potassium iodide and 10 mL of hydrochloric acid. Use sodium thiosulfate standard titration solution to make titration, until the brown color disappears. Do a blank test at the same time. A.6.3 Result calculation ......