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GA/T 1634-2019: Forensic sciences - Examination methods for four amphetamines including amphetamine in hair and blood samples - GC and GC-MS
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Forensic sciences - Examination methods for four amphetamines including amphetamine in hair and blood samples - GC and GC-MS
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GA/T 1634-2019
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Basic data | Standard ID | GA/T 1634-2019 (GA/T1634-2019) | | Description (Translated English) | Forensic sciences - Examination methods for four amphetamines including amphetamine in hair and blood samples - GC and GC-MS | | Sector / Industry | Public Security (Police) Industry Standard (Recommended) | | Classification of Chinese Standard | A92 | | Classification of International Standard | 13.310 | | Word Count Estimation | 18,184 | | Date of Issue | 2019 | | Date of Implementation | 2019-12-01 | | Issuing agency(ies) | Ministry of Public Security | GA/T 1634-2019: Forensic sciences - Examination methods for four amphetamines including amphetamine in hair and blood samples - GC and GC-MS
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Forensic sciences - Examination methods for four amphetamines including amphetamine in hair and blood samples - GC and GC-MS
ICS 13.310
A92
Public Safety Industry Standard of the People's Republic of China
Forensic hair, amphetamine in blood, etc.
Four kinds of amphetamine drugs test
Gas chromatography and gas chromatography-mass spectrometry
Published on October 14,.2019
2019-12-01 Implementation
Issued by the Ministry of Public Security of the People's Republic of China
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
Please note that some content of this document may involve patents. The issuer of this document does not assume responsibility for identifying these patents.
This standard was proposed by the National Toxic Analysis Sub-Committee of Criminal Technology Standardization Technical Committee (SAC/TC179/SC1) and
Be in charge.
This standard was drafted by. Material Evidence Appraisal Center of the Ministry of Public Security, Material Evidence Appraisal Center of Shanghai Public Security Bureau.
The main drafters of this standard. Zhu Jun, Liu Yao, Yu Zhongshan, Chang Jing, Song Ge, Zhang Yurong, Wang Rong, Wang Ruihua.
Forensic hair, amphetamine in blood, etc.
Four kinds of amphetamine drugs test
Gas chromatography and gas chromatography-mass spectrometry
1 Scope
This standard stipulates forensic hair, amphetamine (AM), methamphetamine (deoxyephedrine, MA), 3,4-methylenedioxy in the blood
Qualitative and quantitative test method and gas phase of gas chromatography (GC) for methylmethamphetamine (MDMA) and 3,4-methylenedioxyamphetamine (MDA)
Chromatography-mass spectrometry (GC-MS) qualitative and quantitative test method.
This standard applies to forensic hair, amphetamine, methamphetamine, 3,4-methylenedioxymethamphetamine and 3,4-methylene
Qualitative and quantitative analysis of dioxyamphetamine. Other suspicious samples of amphetamine, methamphetamine, 3,4-methylenedioxymethamphetamine
The qualitative analysis and quantitative analysis of amine and 3,4-methylenedioxyamphetamine can be used by reference.
2 Normative references
The following documents are essential for the application of this document. For dated reference documents, only the dated version applies to this article
Pieces. For the cited documents without date, the latest version (including all amendments) applies to this document.
GB/T 6682 Analysis of laboratory water specifications and test methods
GA/T 122 Nomenclature of poison analysis
3 Terms and definitions
The terms and definitions defined in GA/T 122 apply to this document.
4 Principle
Using blank samples and added samples as controls, extract, purify, concentrate and derive hair and blood samples according to the requirements of parallel operation
Qualitative quantitative analysis by gas chromatography, gas chromatography-mass spectrometry, and the retention time and mass spectrum of each component of the target or its derivative products
The characteristic ion fragment peak and relative abundance ratio are used as the basis for qualitative judgment; the peak area is used as the quantitative basis, and the external standard method or the internal standard method is used for quantification
analysis.
5 Reagents and materials
5.1 Reagents
The water used for the experiment shall conform to the tertiary water specified in GB/T 6682.Unless otherwise stated, the reagents used in the analysis are of analytical grade,
Reagents include.
a) Internal standard 4-phenylbutylamine (4-PBA) or other equivalent internal standard;
b) methanol;
c) ethanol;
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