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SN/T 2235-2008 English PDF

Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
SN/T 2235-2008719 Add to Cart 3 days Determination of cyprodinil residues in food for import and export. GC-MS method Obsolete

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Basic data

Standard ID: SN/T 2235-2008 (SN/T2235-2008)
Description (Translated English): Determination of cyprodinil residues in food for import and export. GC-MS method
Sector / Industry: Commodity Inspection Standard (Recommended)
Classification of Chinese Standard: X04
Word Count Estimation: 18,121
Date of Issue: 2008-11-18
Date of Implementation: 2009-06-01
Regulation (derived from): National Quality Inspection [2008] No. 577
Issuing agency(ies): General Administration of Customs
Summary: This standard specifies the food cyprodinil residues by gas chromatography mass spectrometry detection and confirmation methods. This standard applies to rice, soybeans, small cabbage, sweet peas, pears, citrus, peanuts, tea, beef, chicken, shrimp, honey cyprodinil residues detection and confirmation.

SN/T 2235-2008: Determination of cyprodinil residues in food for import and export. GC-MS method

---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
Determination of cyprodinil residues in food for import and export.GC-MS method Exit inspection and quarantine industry standard book People's Republic of China Imported and exported food cyprodinil Residue Detection Gas chromatography - mass spectrometry Posted 2008-11-18 2009-06-01 implementation People's Republic of China The State Administration of Quality Supervision, Inspection and Quarantine released

Foreword

Appendix A of this standard is an informative annex. This standard is proposed and managed by the National Certification and Accreditation Administration Committee. This standard was drafted. People's Republic of China Zhejiang Exit Inspection and Quarantine, People's Republic of China Liaoning Entry-Exit Inspection and Quarantine Bureau. The main drafters of this standard. Ding Huiying, Xie, Chen Xiaomei, will Xiaoying, Zhou Xu, Yao Liang, Wei Feng. This standard is the first release of the entry-exit inspection and quarantine industry standards. Imported and exported food cyprodinil Residue Detection Gas chromatography - mass spectrometry

1 Scope

This standard specifies the foods cyprodinil residues by gas chromatography - mass spectrometry detection and confirmation methods. This standard applies to rice, soybeans, small cabbage, sweet peas, pears, oranges, peanuts, tea, beef, chicken, shrimp, honey cyprodinil Residue detection and confirmation.

2 Method summary

Sample remaining cyprodinil with hexane - acetone (1 + 1) extraction by gel permeation chromatography column and propylsulfonyl silyl silica Yang Ion exchange column purification, gas chromatography - mass spectrometry and confirmed, external standard.

3 Reagents and materials

Unless otherwise stated, the use of organic reagents were HPLC grade water as distilled water. 3.1 n-hexane. 3.2 acetone. 3.3 cyclohexane. 3.4 ethyl acetate. 3.5 methanol. 3.6 ammonia. AR. 3.7 hydrochloric acid. AR. 3.8 0.1mol/L hydrochloric acid solution. take 9mL amount of hydrochloric acid, diluted with an appropriate amount of water to 1000mL. 3.9 Sodium chloride. AR. 3.10 Anhydrous sodium sulfate. AR, 650 ℃ burning 4h, cooled in a desiccator to room temperature and stored in a sealed bottle aside. 3.11 propylsulfonyl silyl silica gel cation-exchange column. 3mL, 500mg or equivalent person. 3.12 cyprodinil (Cyprodinil) standard substance. purity of greater than 99%, of the formula. C14H15N3 Molecular Weight. 225.3CAS No. 121552-61-2. 3.13 cyprodinil standard solution. Accurately weigh an adequate amount of cyprodinil standard material with acetone dubbed the concentration of 100μg/mL standard Stock solution. If necessary with acetone diluted to the appropriate concentration of the working standard solution. Standard stock solution at 0 ℃ ~ 4 ℃ refrigerator to save, effective Period of 12 months, working standard solution stored at 0 ℃ ~ 4 ℃ refrigerator for a period of six months.

4 instruments and equipment

4.1 Gas chromatography - mass spectrometry. source with electron impact (EI). 4.2 vortex mixer. 4.3 centrifuge. speed is greater than 5000r/min. 4.4 nitrogen blowing instrument. 4.5 rotary evaporator. 4.6 homogenizer. 4.7 Solid phase extraction device. 4.8 Multifunction food mixer. 4.9 mill.
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