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GA/T 2025-2023 English PDF

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GA/T 2025-2023: Forensic sciences - Examination methods for 5-MeO-DiPT and 5-MeO-MiPT in suspected drugs - LC and LC-MS
Status: Valid
Standard IDUSDBUY PDFLead-DaysStandard Title (Description)Status
GA/T 2025-2023279 Add to Cart 3 days Forensic sciences - Examination methods for 5-MeO-DiPT and 5-MeO-MiPT in suspected drugs - LC and LC-MS Valid

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Basic data

Standard ID: GA/T 2025-2023 (GA/T2025-2023)
Description (Translated English): Forensic sciences - Examination methods for 5-MeO-DiPT and 5-MeO-MiPT in suspected drugs - LC and LC-MS
Sector / Industry: Public Security (Police) Industry Standard (Recommended)
Classification of Chinese Standard: A92
Classification of International Standard: 13.310
Word Count Estimation: 14,146
Date of Issue: 2023-03-01
Date of Implementation: 2023-12-01
Issuing agency(ies): Ministry of Public Security

GA/T 2025-2023: Forensic sciences - Examination methods for 5-MeO-DiPT and 5-MeO-MiPT in suspected drugs - LC and LC-MS


---This is a DRAFT version for illustration, not a final translation. Full copy of true-PDF in English version (including equations, symbols, images, flow-chart, tables, and figures etc.) will be manually/carefully translated upon your order.
ICS 13.310 CCSA92 Public safety industry standards of the People's Republic of China Forensic Science Suspected Drugs 5-MeO-DiPT and 5-MeO-MiPT test Liquid Chromatography and Liquid Chromatography-Mass Spectrometry Published on 2023-03-01 Implemented on 2023-12-01 Released by the Ministry of Public Security of the People's Republic of China

Foreword

This document complies with the provisions of GB/T 1.1-2020 "Standardization Work Guidelines Part 1.Structure and Drafting Rules of Standardization Documents" Drafting. Please note that some content in this document may be subject to patents. The publisher of this document assumes no responsibility for identifying patents. This document is proposed and submitted by the Toxic Analysis Sub-Technical Committee of the National Technical Committee for Standardization of Criminal Technology (SAC/TC179/SC1). Return to home. This document was drafted by. Identification Center of the Ministry of Public Security, Physical Evidence Identification Center of the Jilin Provincial Public Security Department, and Anti-Narcotics Intelligence Technology Center of the Ministry of Public Security. The main drafters of this document. Yang Hongxian, Zhao Yanbiao, Qian Zhenhua, Zheng Hui, Zhang Chunshui, Sun Jilai, Chen Jing, Zhao Yang, Chang Ying, Li Peng, Wang Dan, Zheng Xiaoyu, Wen Wu, Zhai Wanfeng, Liu Kelin, Gao Lisheng. Forensic Science Suspected Drugs 5-MeO-DiPT and 5-MeO-MiPT test Liquid Chromatography and Liquid Chromatography-Mass Spectrometry

1 Scope

This document describes 5-methoxy-N,N-diisopropyltryptamine (5-MeO-DiPT) and N-methyl- Liquid chromatography-mass spectrometry (LC-MS) qualitative detection method and liquid chromatography (LC) quantification of N-isopropyl-5-methoxytryptamine (5-MeO-MiPT) Testing method. This document is applicable to the qualitative and quantitative analysis of 5-MeO-DiPT and 5-MeO-MiPT in suspected drugs in the field of forensic science.

2 Normative reference documents

The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, the dated quotations For undated referenced documents, only the version corresponding to that date applies to this document; for undated referenced documents, the latest version (including all amendments) applies to this document. GB/T 6682 Specifications and test methods for water used in analytical laboratories GB/T 27418 Evaluation and expression of measurement uncertainty GA/T 122 Toxicological analysis terminology

3 Terms and definitions

The terms and definitions defined in GA/T 122 apply to this document.

4 Principles

Extract 5-MeO-DiPT and 5-MeO-MiPT from suspected drugs (see Appendix A for compound information). Using liquid chromatography-mass Spectral detection is based on retention time, mass spectrum characteristic ion pairs and ion pair abundance ratios as the basis for qualitative judgment; liquid chromatography is used for detection, using color The peak area of the spectrum was used as the basis for quantitative analysis, and the external standard single point method or the external standard standard curve method was used for quantitative analysis.

5 Reagents and materials

5.1 Reagents The experimental water should comply with the first-class water specified in GB/T 6682.The reagents used in the analysis were all chromatographically pure. Includes the following reagents. a) Acetonitrile. b) methanol. c) Formic acid-ammonium acetate buffer (take the preparation of 1000mL as an example). Weigh 154mg of ammonium acetate, dissolve it in water, and add 1.0mL of ammonium acetate. Dilute the acid to 1000mL with water, filter it with a vacuum filtration pump, and sonicate it with an ultrasonic cleaner before use. d) 0.1% formic acid methanol solution (taking 1000mL as an example). Measure 1.0mL formic acid, dissolve it in methanol and dilute to volume
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