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YB/T 105-2014 PDF English

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YB/T 105-2014: Methods of physical testing for metallurgical lime
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YB/T 105: Evolution and historical versions

Standard IDContents [version]USDSTEP2[PDF] deliveryName of Chinese StandardStatus
YB/T 105-2014English150 Add to Cart 0-9 seconds. Auto-delivery Methods of physical testing for metallurgical lime Valid
YB/T 105-2005English239 Add to Cart 2 days Methods of physical testing for metallurgical quicklime Obsolete
YB/T 105-1997English239 Add to Cart 2 days Methods of physical testing for metallurgical quicklime Obsolete

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YB/T 105-2014: Methods of physical testing for metallurgical lime

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YB FERROUS METALLURGICAL INDUSTRY STANDARD ICS 73.080 D 52 Replacing YB/T 105-2005 Methods of physical testing for metallurgical lime Issued on. MAY 06, 2014 Implemented on. OCTOBER 01, 2014 Issued by. Ministry of Industry and Information Technology of PRC

Table of Contents

Foreword... 3 1 Scope... 4 2 Normative references... 4 3 Terms and definitions... 4 4 Activity testing methods... 5 5 Particle size test method... 8 Appendix A (Normative) Acceptance procedure flow chart of specimen analysis result ... 10

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard replaces YB/T 105-2005 "Methods of physical testing for metallurgical lime". Compared with YB/T 105-2005, this standard has the following modifications. - ADD reactivity potentiometric titration detection; - MODIFY the definition; - MODIFY the calculation of inspection results; - MODIFY the allowable error of inspection results; - ADD the Appendix A (normative). This standard was proposed by the China Iron and Steel Industry Association. This standard shall be under the jurisdiction of the National Steel Standardization Technical Committee (SAC/TC 183). Drafting organizations of this standard. Shougang Corporation, Metallurgical Industry Information Standards Research Institute, Anshan Kexiang Instrument Co., Ltd., Shaoxing Hongchi Machinery Instrument Manufacturing Co., Ltd. The main drafters of this standard. Wu Chaohui, Li Songtian, Zhang Lei, Kong Zhigang, Qiu Jinhui, Gao Jianping, Wang Jiangwei. This standard replaces the standard previously issued as follows. - ZBQ 27002-1985, YB/T 105-1997, YB/T 105-2005. Methods of physical testing for metallurgical lime Warning. Personnel to whom this standard applies shall have practical experience in formal laboratory work. This standard does not address all possible safety issues. Users are responsible for taking appropriate safety and health measures and ensuring compliance with the conditions stipulated in relevant national regulations.

1 Scope

This standard specifies the terms and definitions, method principles, test methods, calculation of results for the determination of reactivity and particle size composition of metallurgical lime. This standard is applicable to the determination of reactivity and particle size composition of metallurgical lime.

2 Normative references

The following documents are essential to the application of this document. For the dated documents, only the versions with the dates indicated are applicable to this document; for the undated documents, only the latest version (including all the amendments) is applicable to this standard. GB/T 2007.7 General rules for the sampling and sample preparation of minerals in bulk. The method for determination of size by manual sieving GB/T 6003.2 Test sieves of perforated metal plate GB/T 8170 Rules of rounding off for numerical values & expression and judgement of limiting values

3 Terms and definitions

The following terms and definitions apply to this document. Reactivity The reaction rate of lime hydration, which is expressed as the number of milliliters of 4 mol/L hydrochloric acid consumed in 10 minutes.

4 Activity testing methods

4.1 Principle Hydrate a certain amount of the specimen. At the same time, use a certain concentration of hydrochloric acid, to neutralize the calcium hydroxide produced during the lime hydration process. 4.2 Reagents 4.2.1 Hydrochloric acid (4 mol/L). 4.2.2 Phenolphthalein indicator solution (5 g/L). Weigh 0.5 g of phenolphthalein. Add 50 mL of ethanol to dissolve. Add water to dilute it to 100 mL. 4.3 Test equipment and tools 4.3.1 Jaw crusher 60 mm × 100 mm. 4.3.2 Sampling sieve. 1 mm and 5 mm round hole sieve. 4.3.3 Ground mouth bottle. 500 mL. 4.3.8 Dryer. The diameter is 250 mm. 4.3.9 Beaker. 3000 mL. 4.3.10 Graduated cylinder. 2000 mL. 4.3.11 Burette. 500 mL, minimum scale not larger than 1 mL. 4.3.12 Thermometer. The maximum temperature is 100 °C; the scale is not greater than 1 °C. 4.3.13 Dropper bottle. 50 mL. 4.3.14 Stopwatch (or timer). 4.3.15 Stirrer. 4.3.15.1 The power is not less than 100 W. 4.3.16 Metallurgical lime reactivity automatic detector 4.3.16.1 Timing accuracy. 0.5 s. 4.3.16.2 Liquid level meter measurement accuracy. 0.05%. 4.3.16.3 Titration accuracy. 0.5 mL. 4.3.16.4 pH value detector. 0 ~ 14, resolution 0.01. 4.3.16.5 Mixer speed. 250 r/min ~ 300 r/min. 4.3.16.6 Equipped with constant temperature water outlet. 4.4 Specimen 4.4.1 Specimen size Follow the provisions of YB/T 042. 4.4.2 Specimen preparation method Crush the sample, until it passes through a 5 mm sieve. Then use a 1 mm sieve to remove the fine powder. Mix thoroughly and separate out about 500 g using the sample reduction method. Store it in a labeled ground-mouth bottle, for later use. 4.5 Test procedures 4.5.2 Automatic hydrochloric acid titration method 4.5.2.1 Turn on the hot water heater. (After the temperature reaches the requirement) automatically inject 2000 mL of 40 °C ± 1 °C hot water, into the 3000 mL beaker. 4.5.2.2 Start the equipment and the stirring paddle will turn on automatically. The system enters the test state. The pH value detector detects the pH value. It controls the pH value to 7.0 ± 0.1. 4.6 Calculation of results 4.6.1 If the results of two independent measurements of the same specimen are not greater than the allowable difference (see 4.6.2), THEN take the arithmetic mean as the test result. If the results of two independent measurements are greater than the allowable difference, increase the number of tests and determine the test results as specified in Appendix A. The test results are rounded to integers, in accordance with GB/T 8170. 4.6.2 Allowable difference The absolute value of the difference -- between two independent measurement results of the same specimen -- shall not be greater than 4% of the average value.

5 Particle size test method

5.1 Key points of method The specimens are classified for particle size, according to the prescribed sieve mesh and operating methods. The test results are expressed as the percentage of the quality of each particle size. 5.2 Test equipment and tools 5.2.1 Square hole sieve. The sieve hole specifications and size deviations comply with GB/T 6003.The size of the sieve surface is approximately 800 mm × 600 mm; the height of the sieve frame is approximately 120 mm; handles are installed at both ends of the sieve frame. 5.3 Specimens Follow the provisions of YB/T 042. 5.4 Screening steps 5.4.1 The specimen is screened from large holes to small holes. The height of the sieve from the ground, steel plate or receiving plate shall not exceed 200 mm. 5.4.5 Combine the material above the sieve into the picked lime blocks. Use the same method for the lime under sieve, to continue to sieve it on the smaller sieve in the selected series of sieves. The following is same, until the screening is completed. 5.4.6 The screening end point shall be implemented, in accordance with the relevant provisions of GB/T 2007.7. 5.4.7 Weigh and record the various levels of screened lime products. 5.5 Result calculation Add up the mass of each level of lime samples. The difference -- between the total mass and the mass of the original specimen -- shall be within 1.5% of the mass of the original specimen. Otherwise, the test will be invalid. Loss of lime is calculated at the smallest level. 5.6 Allowable difference See Table 1, for allowable differences. YB/T 105-2014 YB FERROUS METALLURGICAL INDUSTRY STANDARD ICS 73.080 D 52 Replacing YB/T 105-2005 Methods of physical testing for metallurgical lime Issued on. MAY 06, 2014 Implemented on. OCTOBER 01, 2014 Issued by. Ministry of Industry and Information Technology of PRC

Table of Contents

Foreword... 3 1 Scope... 4 2 Normative references... 4 3 Terms and definitions... 4 4 Activity testing methods... 5 5 Particle size test method... 8 Appendix A (Normative) Acceptance procedure flow chart of specimen analysis result ... 10

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009. This standard replaces YB/T 105-2005 "Methods of physical testing for metallurgical lime". Compared with YB/T 105-2005, this standard has the following modifications. - ADD reactivity potentiometric titration detection; - MODIFY the definition; - MODIFY the calculation of inspection results; - MODIFY the allowable error of inspection results; - ADD the Appendix A (normative). This standard was proposed by the China Iron and Steel Industry Association. This standard shall be under the jurisdiction of the National Steel Standardization Technical Committee (SAC/TC 183). Drafting organizations of this standard. Shougang Corporation, Metallurgical Industry Information Standards Research Institute, Anshan Kexiang Instrument Co., Ltd., Shaoxing Hongchi Machinery Instrument Manufacturing Co., Ltd. The main drafters of this standard. Wu Chaohui, Li Songtian, Zhang Lei, Kong Zhigang, Qiu Jinhui, Gao Jianping, Wang Jiangwei. This standard replaces the standard previously issued as follows. - ZBQ 27002-1985, YB/T 105-1997, YB/T 105-2005. Methods of physical testing for metallurgical lime Warning. Personnel to whom this standard applies shall have practical experience in formal laboratory work. This standard does not address all possible safety issues. Users are responsible for taking appropriate safety and health measures and ensuring compliance with the conditions stipulated in relevant national regulations.

1 Scope

This standard specifies the terms and definitions, method principles, test methods, calculation of results for the determination of reactivity and particle size composition of metallurgical lime. This standard is applicable to the determination of reactivity and particle size composition of metallurgical lime.

2 Normative references

The following documents are essential to the application of this document. For the dated documents, only the versions with the dates indicated are applicable to this document; for the undated documents, only the latest version (including all the amendments) is applicable to this standard. GB/T 2007.7 General rules for the sampling and sample preparation of minerals in bulk. The method for determination of size by manual sieving GB/T 6003.2 Test sieves of perforated metal plate GB/T 8170 Rules of rounding off for numerical values & expression and judgement of limiting values

3 Terms and definitions

The following terms and definitions apply to this document. Reactivity The reaction rate of lime hydration, which is expressed as the number of milliliters of 4 mol/L hydrochloric acid consumed in 10 minutes.

4 Activity testing methods

4.1 Principle Hydrate a certain amount of the specimen. At the same time, use a certain concentration of hydrochloric acid, to neutralize the calcium hydroxide produced during the lime hydration process. 4.2 Reagents 4.2.1 Hydrochloric acid (4 mol/L). 4.2.2 Phenolphthalein indicator solution (5 g/L). Weigh 0.5 g of phenolphthalein. Add 50 mL of ethanol to dissolve. Add water to dilute it to 100 mL. 4.3 Test equipment and tools 4.3.1 Jaw crusher 60 mm × 100 mm. 4.3.2 Sampling sieve. 1 mm and 5 mm round hole sieve. 4.3.3 Ground mouth bottle. 500 mL. 4.3.8 Dryer. The diameter is 250 mm. 4.3.9 Beaker. 3000 mL. 4.3.10 Graduated cylinder. 2000 mL. 4.3.11 Burette. 500 mL, minimum scale not larger than 1 mL. 4.3.12 Thermometer. The maximum temperature is 100 °C; the scale is not greater than 1 °C. 4.3.13 Dropper bottle. 50 mL. 4.3.14 Stopwatch (or timer). 4.3.15 Stirrer. 4.3.15.1 The power is not less than 100 W. 4.3.16 Metallurgical lime reactivity automatic detector 4.3.16.1 Timing accuracy. 0.5 s. 4.3.16.2 Liquid level meter measurement accuracy. 0.05%. 4.3.16.3 Titration accuracy. 0.5 mL. 4.3.16.4 pH value detector. 0 ~ 14, resolution 0.01. 4.3.16.5 Mixer speed. 250 r/min ~ 300 r/min. 4.3.16.6 Equipped with constant temperature water outlet. 4.4 Specimen 4.4.1 Specimen size Follow the provisions of YB/T 042. 4.4.2 Specimen preparation method Crush the sample, until it passes through a 5 mm sieve. Then use a 1 mm sieve to remove the fine powder. Mix thoroughly and separate out about 500 g using the sample reduction method. Store it in a labeled ground-mouth bottle, for later use. 4.5 Test procedures 4.5.2 Automatic hydrochloric acid titration method 4.5.2.1 Turn on the hot water heater. (After the temperature reaches the requirement) automatically inject 2000 mL of 40 °C ± 1 °C hot water, into the 3000 mL beaker. 4.5.2.2 Start the equipment and the stirring paddle will turn on automatically. The system enters the test state. The pH value detector detects the pH value. It controls the pH value to 7.0 ± 0.1. 4.6 Calculation of results 4.6.1 If the results of two independent measurements of the same specimen are not greater than the allowable difference (see 4.6.2), THEN take the arithmetic mean as the test result. If the results of two independent measurements are greater than the allowable difference, increase the number of tests and determine the test results as specified in Appendix A. The test results are rounded to integers, in accordance with GB/T 8170. 4.6.2 Allowable difference The absolute value of the difference -- between two independent measurement results of the same specimen -- shall not be greater than 4% of the average value.

5 Particle size test method

5.1 Key points of method The specimens are classified for particle size, according to the prescribed sieve mesh and operating methods. The test results are expressed as the percentage of the quality of each particle size. 5.2 Test equipment and tools 5.2.1 Square hole sieve. The sieve hole specifications and size deviations comply with GB/T 6003.The size of the sieve surface is approximately 800 mm × 600 mm; the height of the sieve frame is approximately 120 mm; handles are installed at both ends of the sieve frame. 5.3 Specimens Follow the provisions of YB/T 042. 5.4 Screening steps 5.4.1 The specimen is screened from large holes to small holes. The height of the sieve from the ground, steel plate or receiving plate shall not exceed 200 mm. 5.4.5 Combine the material above the sieve into the picked lime blocks. Use the same method for the lime under sieve, to continue to sieve it on the smaller sieve in the selected series of sieves. The following is same, until the screening is completed. 5.4.6 The screening end point shall be implemented, in accordance with the relevant provisions of GB/T 2007.7. 5.4.7 Weigh and record the various levels of screened lime products. 5.5 Result calculation Add up the mass of each level of lime samples. The difference -- between the total mass and the mass of the original specimen -- shall be within 1.5% of the mass of the original specimen. Otherwise, the test will be invalid. Loss of lime is calculated at the smallest level. 5.6 Allowable difference See Table 1, for allowable differences. ......
Source: Above contents are excerpted from the full-copy PDF -- translated/reviewed by: www.ChineseStandard.net / Wayne Zheng et al.


      

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