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JJF 1800-2020 PDF English

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JJF 1800-2020: Calibration specification of aerosol photometers
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JJF 1800-2020: Calibration specification of aerosol photometers

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JJF METROLOGY SPECIFICATION OF THE PEOPLE’S REPUBLIC OF CHINA Calibration Specification for Aerosol Photometers Issued on. JANUARY 17, 2020 Implemented on. APRIL 17, 2020 Issued by. State Administration for Market Regulation Administrative organization. National Technical Committee on Environmental Stoichiometry Main drafting organizations. Shanghai Institute of Metrology and Testing Technology Qingdao Metrology Technology Research Institute China Institute of Metrology Participating drafting organizations. Shanghai Environmental Protection Product Quality Supervision and Inspection Station Shenyang Jiaye Scientific Instrument Co., Ltd. Suzhou Huayu Purification Equipment Co., Ltd. This specification is entrusted to the National Environmental Chemical Metrology Technical Committee to be responsible for the interpretation. Calibration Specification for Aerosol Photometers Main drafters of this Specification. Zhang Ailiang (from Shanghai Institute of Metrology and Testing Technology) Xia Chun (from Qingdao Metrology Technology Research Institute) Liu Yue (from Shanghai Institute of Metrology and Testing Technology) Liu Junjie (from China Institute of Metrology) Participating drafters. Shi Chanzhen (from Shanghai Environmental Protection Product Quality Supervision and Inspection Station) Li Hefeng (from Shenyang Jiaye Scientific Instrument Co., Ltd.) Gao Zheng (from Suzhou Huayu Purification Equipment Co., Ltd.)

Table of Contents

Introduction... 5 1 Scope... 6 2 Terms... 6 3 Overview... 6 4 Metrology characteristics... 7 5 Calibration conditions... 7 5.1 Environmental conditions... 7 5.2 Metrology standard instruments... 8 6 Calibration items and calibration methods... 8 6.1 Preparation before calibration... 8 6.2 Calibration items... 8 7 Calibration result expression... 12 7.1 Calibration record... 12 7.2 Processing of calibration results... 12 8 Recalibration time interval... 13 Annex A Calibration method for concentration indication error of precision aerosol photometer... 14 Annex B Examples for measurement uncertainty evaluation of mass concentration indication error of precision aerosol photometer... 18 Annex C Examples for uncertainty evaluation of indication error of mass concentration of aerosol photometer... 25 Annex D Raw recording format for aerosol photometer calibration (reference)... 31 Annex E Aerosol photometer calibration certificate (inner page) format (reference) 33

Introduction

This Specification is prepared based on JJF 1071-2010 "The rules for drafting national calibration specification", JJF 1001-2011 "General Terms in Metrology and Their Definitions" and JJF 1059.1-2012 "Evaluation and Expression of Uncertainty in Measurement". The technical indicators of this Specification refer to IEST-RP-CC013.3-2012 "Calibration procedures and guidelines for select equipment used in testing cleanrooms and other controlled environments". This Specification is issued for the first time. Calibration Specification for Aerosol Photometers

1 Scope

This Specification applies to the calibration of light scattering principle aerosol photometers with a measurement range of (0.01~100) μg/L. The aerosol photometers with other measuring ranges can be calibrated with reference to this Specification.

2 Terms

PAO-4 aerosol Aerosol refers to a colloidal dispersion system formed by solid or liquid small particles dispersed and suspended in a gas medium. It is also called as gas dispersion system. Its dispersion phase is solid, liquid or solid-liquid mixture. PAO-4 aerosol in this Specification refers to polydisperse aerosol, which takes poly-alpha-olefin oil (PAO) with a kinematic viscosity of 4m2/s as the generating medium and is generated by the fog mixing device of the aerosol photometer.

3 Overview

Aerosol photometer (hereinafter referred to as the instrument) is an instrument used to measure the leakage rate of high-efficiency filters and the leakage rate of high- efficiency filtration systems installed with high-efficiency filters.

4 Metrology characteristics

4.1 Sampling flow indication error. no more than ±5%. 4.2 Sampling flow repeatability. not more than 2%. 4.3 Sampling flow stability. sampling flow is not more than 5% within 1h.

5 Calibration conditions

5.1 Environmental conditions 5.1.1 Temperature. (15~30)℃. Relative humidity. ≤85%. 5.2 Metrology standard instruments 5.2.1 Precision aerosol photometer. the maximum allowable error of mass concentration does not exceed ±10%; 5.2.2 Flow standard device. the measurement range is (0~50)L/min; the maximum allowable error does not exceed ±1.0%.

6 Calibration items and calibration methods

6.1 Preparation before calibration Connect the calibrated instrument, precision aerosol photometer and aerosol fog mixing device as required. According to the use requirements of each equipment, the normal operation of preheating shall not be less than 10min. 6.2 Calibration items 6.2.2 Flow repeatability According to the connection method in 6.2.1, read the standard flow value after the instrument is stable. Repeat the measurement 6 times. Calculate the sampling flow repeatability according to formula (2).

7 Calibration result expression

7.1 Calibration record Refer to Annex D for the calibration record format. 7.2 Processing of calibration results Calibration results shall be reflected on the calibration certificate or calibration report. The calibration certificate or report includes at least the following information.

8 Recalibration time interval

The recalibration time interval of the instrument shall be determined by the user according to the usage of the instrument, the performance of the instrument itself, and so on. JJF METROLOGY SPECIFICATION OF THE PEOPLE’S REPUBLIC OF CHINA Calibration Specification for Aerosol Photometers Issued on. JANUARY 17, 2020 Implemented on. APRIL 17, 2020 Issued by. State Administration for Market Regulation Administrative organization. National Technical Committee on Environmental Stoichiometry Main drafting organizations. Shanghai Institute of Metrology and Testing Technology Qingdao Metrology Technology Research Institute China Institute of Metrology Participating drafting organizations. Shanghai Environmental Protection Product Quality Supervision and Inspection Station Shenyang Jiaye Scientific Instrument Co., Ltd. Suzhou Huayu Purification Equipment Co., Ltd. This specification is entrusted to the National Environmental Chemical Metrology Technical Committee to be responsible for the interpretation. Calibration Specification for Aerosol Photometers Main drafters of this Specification. Zhang Ailiang (from Shanghai Institute of Metrology and Testing Technology) Xia Chun (from Qingdao Metrology Technology Research Institute) Liu Yue (from Shanghai Institute of Metrology and Testing Technology) Liu Junjie (from China Institute of Metrology) Participating drafters. Shi Chanzhen (from Shanghai Environmental Protection Product Quality Supervision and Inspection Station) Li Hefeng (from Shenyang Jiaye Scientific Instrument Co., Ltd.) Gao Zheng (from Suzhou Huayu Purification Equipment Co., Ltd.)

Table of Contents

Introduction... 5 1 Scope... 6 2 Terms... 6 3 Overview... 6 4 Metrology characteristics... 7 5 Calibration conditions... 7 5.1 Environmental conditions... 7 5.2 Metrology standard instruments... 8 6 Calibration items and calibration methods... 8 6.1 Preparation before calibration... 8 6.2 Calibration items... 8 7 Calibration result expression... 12 7.1 Calibration record... 12 7.2 Processing of calibration results... 12 8 Recalibration time interval... 13 Annex A Calibration method for concentration indication error of precision aerosol photometer... 14 Annex B Examples for measurement uncertainty evaluation of mass concentration indication error of precision aerosol photometer... 18 Annex C Examples for uncertainty evaluation of indication error of mass concentration of aerosol photometer... 25 Annex D Raw recording format for aerosol photometer calibration (reference)... 31 Annex E Aerosol photometer calibration certificate (inner page) format (reference) 33

Introduction

This Specification is prepared based on JJF 1071-2010 "The rules for drafting national calibration specification", JJF 1001-2011 "General Terms in Metrology and Their Definitions" and JJF 1059.1-2012 "Evaluation and Expression of Uncertainty in Measurement". The technical indicators of this Specification refer to IEST-RP-CC013.3-2012 "Calibration procedures and guidelines for select equipment used in testing cleanrooms and other controlled environments". This Specification is issued for the first time. Calibration Specification for Aerosol Photometers

1 Scope

This Specification applies to the calibration of light scattering principle aerosol photometers with a measurement range of (0.01~100) μg/L. The aerosol photometers with other measuring ranges can be calibrated with reference to this Specification.

2 Terms

PAO-4 aerosol Aerosol refers to a colloidal dispersion system formed by solid or liquid small particles dispersed and suspended in a gas medium. It is also called as gas dispersion system. Its dispersion phase is solid, liquid or solid-liquid mixture. PAO-4 aerosol in this Specification refers to polydisperse aerosol, which takes poly-alpha-olefin oil (PAO) with a kinematic viscosity of 4m2/s as the generating medium and is generated by the fog mixing device of the aerosol photometer.

3 Overview

Aerosol photometer (hereinafter referred to as the instrument) is an instrument used to measure the leakage rate of high-efficiency filters and the leakage rate of high- efficiency filtration systems installed with high-efficiency filters.

4 Metrology characteristics

4.1 Sampling flow indication error. no more than ±5%. 4.2 Sampling flow repeatability. not more than 2%. 4.3 Sampling flow stability. sampling flow is not more than 5% within 1h.

5 Calibration conditions

5.1 Environmental conditions 5.1.1 Temperature. (15~30)℃. Relative humidity. ≤85%. 5.2 Metrology standard instruments 5.2.1 Precision aerosol photometer. the maximum allowable error of mass concentration does not exceed ±10%; 5.2.2 Flow standard device. the measurement range is (0~50)L/min; the maximum allowable error does not exceed ±1.0%.

6 Calibration items and calibration methods

6.1 Preparation before calibration Connect the calibrated instrument, precision aerosol photometer and aerosol fog mixing device as required. According to the use requirements of each equipment, the normal operation of preheating shall not be less than 10min. 6.2 Calibration items 6.2.2 Flow repeatability According to the connection method in 6.2.1, read the standard flow value after the instrument is stable. Repeat the measurement 6 times. Calculate the sampling flow repeatability according to formula (2).

7 Calibration result expression

7.1 Calibration record Refer to Annex D for the calibration record format. 7.2 Processing of calibration results Calibration results shall be reflected on the calibration certificate or calibration report. The calibration certificate or report includes at least the following information.

8 Recalibration time interval

The recalibration time interval of the instrument shall be determined by the user according to the usage of the instrument, the performance of the instrument itself, and so on. ......
Source: Above contents are excerpted from the full-copy PDF -- translated/reviewed by: www.ChineseStandard.net / Wayne Zheng et al.


      

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